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Title reduced time hplc analyses for fast quality control ofcitrusessential oils
Journal journal of essential oil research
Year 2015
DOI 10.1080/10412905.2015.1027419
Cited By 34
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Abstract
cold-pressed citrus essential oils contain variable amounts of oxygen heterocyclic compounds highly characteristic of each species. their distribution has been defined by high-performance liquid chromatography (hplc) analysis with an average time of about 45 minutes. here are two methods proposed, applying the latest generation hplc columns based on the fused-core technology. the first method allows the complete resolution of thirty-eight components for a rugged and validated quantitative determination of the oxygen heterocyclic compounds in cold pressed lemon, lime, bergamot grapefruit, sweet orange, bitter orange and mandarin oils, in 10 minutes of total analysis time. the second method is a compromise between chromatographic resolution and analysis time and allows a fingerprinting of each of the abovementioned oils to be obtained, useful for unveiling possible contaminations and frauds in about 3 minutes. this last method can be applied in routine analysis to save time and solvent. the components are sufficiently separated in all the citrus cold pressed oils, permitting detailed profiles of each oil to be acquired and possible contaminations and frauds to be detected.
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Compounds
Plants
Plant Parts
All Records
CompoundCount
nobiletin4
heptamethoxyflavone4
bergamottin4
bergapten4
tangeretin4
sinensetin3
tetra-o-methyl-scutellarein3
5-geranyloxy-7-methoxy-coumarin3
citropten3
osthol2
5-isopentenyloxy-7-methoxy-coumarin2
8-geranyloxy-psoralen2
byakangelicin2
byakangelicol2
cnidicin2
herniarin2
imperatorin2
isoimperatorin2
oxypeucedanin2
oxypeucedanin hydrate2
epoxybergamottin2
epoxybergamottin hydrate2
isomeranzin2
meranzin2
meranzin hydrate2
5-demethyl-tangeretin1
5-demethyl-nobiletin1
aurapten1
epoxyaurapten1
phellopterin1
hexamethoxyflavone1
cnidilin1
isopimpinellin1
PlantFamily
Citrus aurantifoliarutaceae
Citrus aurantiumrutaceae
Citrus bergamiarutaceae
Citrus deliciosarutaceae
Citrus limonrutaceae
Citrus paradisirutaceae
Citrus sinensisrutaceae
Plant PartCount
PlantCompoundPart%